RESUMO Objetivou-se avaliar propriedades físicas de grãos de genótipos de feijão-caupi. O estudo foi conduzido no Laboratório de Armazenamento e Beneficiamento de Grãos e Sementes no Instituto Federal do Norte de Minas Gerais, em Januária, MG. Os tratamentos utilizados foram 17 linhagens-elite e 11 cultivares de grãos de feijão-caupi. O delineamento experimental foi em blocos casualizados, com quatro repetições. As características avaliadas foram a densidade aparente, ângulo de repouso, massa de 1.000 grãos, forma (esfericidade e circularidade), tamanho (área projetada) dos grãos, teor de água e porosidade da massa de grãos. Os genótipos conferem diferentes tamanhos aos grãos de feijão-caupi, o que influencia na variação da densidade aparente, ângulo de repouso e massa de mil grãos. Não houve diferença estatística entre as médias para as variáveis teor de água e porosidade da massa, entre os genótipos avaliados.

ABSTRACT The present study aimed to evaluate the physical properties of cowpea genotypes grains. The study was conducted at the Laboratory for Storage and Processing of Grains and Seeds at the North Federal Institute of Minas Gerais (IFNMG) in Januária, MG, Brazil. The treatments were composed of 17 elite lines and 11 cultivars of cowpea. The experimental design was in randomized blocks with four replicates. The properties evaluated were bulk density, angle of repose, 1000-grain weight, shape (sphericity and circularity), size (projected area) of the grains, water content, and porosity of the grain mass. The genotypes give different sizes to cowpea beans, which influences the variation of bulk density, angle of repose, and 1000-grain weight. There was no statistical difference among the cowpea genotypes evaluated for water content and mass porosity.

Eugenia punicifolia (Kunth) DC, known as “pedra ume-caá” or “pitanguinha do cerrado”, is popularly used to treat infectious diseases like inflammation, and diabetes. Therefore, this study aimed to develop and validate an analytical method by high-performance liquid chromatography with diode array detector (HPLC-DAD) for the seasonal quantification of gallic acid (GA) and ellagic acid (EA), and to co-validate the method for quantification from the ethanol extract and fractions of the E. punicifolia leaves. Chromatographic separations were performed with a mobile phase gradient of acetonitrile/methanol/water acidified with 0.2% formic acid, a flow of 0.8 mL min 1, detection at 254 nm, and a C18 column (250 × 4.6 mm, 5 µm). Method validation parameters were determined following Brazilian legislation. The HPLC-DAD analytical method developed for the quantification of GA and EA was validated and demonstrated to be selective, linear, precise, accurate, robust, and without matrix effect. Accordingly, it is helpful for the analysis of these tannins in crude ethanol extracts and fractions from E. punicifoila leaves. Thus, our results may be of great help for quality control assessment and standardization of raw materials containing Eugenia punicifolia.